nano-sbcl5/sio2 as an efficient catalyst for one-pot synthesis of 2, 4, 5-trisubstituted imidazoles under solvent- free condition
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abstract
a general synthetic route to the synthesis of imidazoles has been developed using nano sbcl5/sio2 under solvent-free conditions. the multi-component reactions of aldehydes, benzil and ammonium acetate were carried out to afford some trisubstituted imidazole derivatives. this method provides several advantages like simple work-up, environmentally benign, and shorter reaction times along with high yields. the mentioned nano catalyst was investigated by sem, tem and xrd. meanwhile, structures of trisubstituted imidazoles were elucidated by ft-ir, 1h nmr and 13c nmr spectra.
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Journal title:
journal of nanostructuresPublisher: university of kashan
ISSN 2251-7871
volume 2
issue 2 2012
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